Determination of the guaranteed shelf life of high-temperature polyimide carbon fiber reinforced plastic prepreg
Valueva M.I., Zelenina I.V., Nacharkina A.V., Boychuk A.S. Determination of the guaranteed shelf life of high-temperature polyimide carbon fiber reinforced plastic prepreg // Proceedings of VIAM. 2023. No. 10. DOI: 10.18577/2307-6046-2023-0-10-64-81. URL: https://test.viam.ru/en/journal/2023/10/7
Keywords
polymer composite materials, high-temperature carbon fiber reinforced plastics, polyimide binder, prepregs, storage conditions, guaranteed shelf life
Abstract
The influence of conditions and duration of storage on the characteristics of a prepreg based on a melted thermosetting polyimide binder grade VS-51 and high-temperature carbon fiber reinforced plastic based on it are studied. In accordance with the data obtained, the guaranteed shelf life of the prepreg was determined in the temperature range from –(18±5) to +(20±5) °С. The binder, reinforcing carbon filler, prepreg and carbon fiber reinforced plastics were manufactured at the technological base of the NRC «Kurchatov Institute» – VIAM.
Reference list
- VIAM 90 years old: proud of the past, creating the future. Ed. E.N. Kablov. Moscow: NRC “Kurchatov Institute” – VIAM, 2022,168 p.
- Kablov E.N. Trends and guidelines for innovative development of Russia. 3rd ed. Moscow: VIAM, 2015, 720 p.
- Onishchenko G.G., Kablov E.N., Ivanov V.V. Scientific and technological development of Russia in the context of achieving national goals: problems and solutions. Innovatsii, 2020, no. 6 (260), pp. 3–16.
- Startsev V.O., Antipov V.V., Slavin A.V., Gorbovets M.A. Modern domestic polymer composite materials for aviation industry (review). Aviation materials and technologies, 2023, no. 2 (71), paper no. 10. Available at: http://www.journal.viam.ru (accessed: June 21, 2023). DOI: 10.18577/2713-0193-2023-0-2-122-144.
- Sidorina A.I. Multiaxial carbon fabrics in the products of aviation technology (review). Aviation materials and technologies, 2021, no. 3 (64), paper no. 10. Available at: http://www.journal.viam.ru (accessed: June 21, 2023). DOI: 10.18577/2713-0193-2021-0-3-105-116.
- Mukhametov R.R., Petrova A.P. Thermosetting binders for polymer composites (review). Aviacionnye materialy i tehnologii, 2019, no. 3 (56), pp. 48–58. DOI: 10.18577/2071-9140-2019-0-3-48-58.
- Tkachuk A.I., Donetsky K.I., Terekhov I.V., Karavaev R.Yu. The use of thermosetting matrices for the manufacture of polymer composite materials by the non-autoclave molding methods. Aviation materials and technology, 2021, no. 1 (62), paper no. 03. Available at: https://journal.viam.ru (accessed: June 21, 2023). DOI: 10.18577/2713-0193-2021-0-1-22-33.
- Kerber M.L., Vinogradov V.M., Golovkin G.S. et al. Polymer composite materials: structure, properties, technology: textbook. Ed. A.A. Berlin. St. Petersburg: Profession, 2008, 560 p.
- Mikhailin Yu.A. Fibrous polymer composite materials in technology. St. Petersburg: Scientific principles and technologies, 2013, 719 p.
- Raskutin A.E. Russian polymer composite materials of new generation, their exploitation and implementation in advanced developed constructions. Aviacionnye materialy i tehnologii, 2017, no. S, pp. 349–367. DOI: 10.18577/2071-9140-2017-0-S-349-367.
- Vasilevich Yu.V., Gorely K.A., Sakhonenko V.M., Sakhonenko S.V., Malyutin E.V. Mechanics of prepregs – calculation of products made of reinforced composite materials: in 2 parts. Ed. Yu.V. Vasilevich. Minsk: BNTU, 2016, part 1, 295 p.
- Vasilevich Yu.V., Gorely K.A., Sakhonenko V.M., Sakhonenko S.V., Malyutin E.V. Mechanics of prepregs - calculation of products made of reinforced composite materials: in 2 parts. Ed. Yu.V. Vasilevich. Minsk: BNTU, 2016, part 2, 283 p.
- Doumcharieva Zh., Kapan S.S. Automation of the temperature regime of an impregnation installation for producing prepreg. Technical Sciences, ser. 12: Automated control systems in production. Available at: http://www.rusnauka.com/18_NPRT_2017/Tecnic/12_227091.doc.htm (accessed: January 12, 2023).
- Satdinov R.A., Veshkin E.A., Postnov V.I., Strelnikov S.V. On the technology of prepreg production. Klei. Germetiki. Tekhnologii, 2020, no. 4, pp. 26–31.
- Polyakova L.Yu. Control of the technological process of manufacturing prepreg for aircraft products: thesis, Cand. Sc. (Tech.). Ufa: Ufimsk. state aviation tech. univ., 2007, 170 p.
- Gunyaeva A.G., Veshkin E.A., Antyufeeva N.V., Panafidnikova A.N., Efimik V.A. Research of influence of the condensation moisture on carbon fiber plastic prepreg on the basis of solution epoxy binder and PСM on its basis. Trudy VIAM, 2019, no. 9 (81), paper no. 09. Available at: http://www.viam-works.ru (accessed: June 21, 2023). DOI: 10.18577/2307-6046-2019-0-9-80-88.
- Veshkin Е.А., Satdinov R.A., Postnov V.I., Strelnikov S.V. Evaluation of effect of duration and storage condition on the properties of prepreg and PCM based on it. Trudy VIAM, 2017, no. 8, paper no. 10. Available at: http://www.viam-works.ru (accessed: June 21, 2023). DOI: 10.18577/2307-6046-2017-0-8-10-10.
- Veshkin E.A., Postnov V.I., Strelnikov S.V., Abramov P.A., Satdinov R.A. Experience in the application of technological control of semi-finished products from polymer composite materials. Izvestiya Samarskogo nauchnogo tsentra RAN, 2014, vol. 16, no. 6 (2), pp. 393–398.
- Cherfas L.V., Gunyaeva A.G., Komarova O.A., Antyufeeva N.V. The analysis of nanomodified prepreg shelf life by its reactivity at storage. Trudy VIAM, 2016, no. 1 (37), paper no. 12. Available at: http://www.viam-works.ru (accessed: June 21, 2023). DOI: 10.18577/2307-6046-2016-0-1-99-106.
- Cheremukhina I.V. Technologies with controlled separation of binder components and the influence of energy fields for the creation of reinforced plastics with a complex of improved properties: thesis, Dr. Sc. (Tech.). Saratov: Saratov State Tech. Univ.; Moscow: MIREA – Rus. Tech. Univ., 2022, 348 p.
- Savitskiy R.S., Galiullin A.R., Mantusova O.Yu., Veshkin E.A. Valuation of the effect of prepreg storage time on warping and PCM properties based on it. Trudy VIAM, 2023, no. 3 (121), paper no. 05. Available at: http://www.viam-works.ru (accessed: June 21, 2023). DOI: 10.18577/2307-6046-2023-0-3-48-57.
- Valueva M.I., Zelenina I.V., Zharinov M.A., Akhmadieva K.R. World market of high temperature polyimide carbon plastic (review). Trudy VIAM, 2019, no. 12 (84), paper no. 08. Available at: http://www.viam-works.ru (accessed: June 21, 2023). DOI: 10.18577/2307-6046-2019-0-12-67-79.
- Valueva M.I., Zelenina I.V., Zharinov M.A., Haskov M.A. High-temperature carbon fiber reinforced plastics based on a thermosetting polyimide binder. Voprosy materialovedeniya, 2020, no. 3 (103), pp. 89–102. DOI: 10.22349/1994-6716-2020-103-3-89-102.
- Mikhailin Yu.A. Heat-resistant polymers and polymer materials. St. Petersburg: Profession, 2006, 624 p.
- Yang S.-Y. Advance polyimide materials: synthesis, characterization, and applications. 1st ed. Elsevier, 2018, 498 p.
- Cho D., Drzal L.T. Phenylethynyl-terminated polyimide, exfoliated graphite nanoplatelets, and the composites: an overview. Carbon letters, 2016, vol. 19, pp. 1–11.
- Tsampas S., Fernberg P., Joffe R. Development of novel high Tg polyimide-based composites. Part II: Mechanical characterization. Journal of Composite Materials, 2018, vol. 52, no. 2, pp. 261–274.
- Kolpachkov E.D., Vavilova M.I., Kurnosov A.O., Gunyaeva A.G. Fiberglass based on thermosetting polyimide binders. All-Rus. Scientific-technical Conf. “New generation polymer composite materials for civil industries”. Moscow: VIAM, 2020. pp. 31–41.
- Cavano P.J., Winters W.E. Fiber reinforced PMR polyimide composites. Washington, D.C.: NASA Lewis Researcher Center, 1978, 105 p.
- Alston W.B. Shelf life of PMR Polyimide monomer solutions and prepregs extended. NASA. Research and Technology, 1999. Available at: https://ntrs.nasa.gov/citations/20050192224 (accessed: January 12, 2023).
- Avimid®R Polyimide Composite. Available at: https://matweb.com/search/datasheettext.aspx?matguid=3dcb6c37bd39469c8e92b27045a13ea4 (accessed: January 12, 2023).
- Avimid®RB Polyimide Composite. Available at: https://www.matweb.com/search/datasheettext.aspx?matguid=d3d9f6997a2145d087bfc9342a8ee61b (accessed: January 12, 2023).
- CYCOM®2237 Polyimide Resin System. Available at: https://www.solvay.com/en/product/cycom-2237 (accessed: July 07, 2023).
- Aerospace. Advance Composite Materials Selector Guide. Available at: https://www.toraytac.com/media/ca3eea73-6961-4ea8-adc7-5d1b861684f6/Bxgrfg/TAC/Documents/Selector%20Guides/Toray Advanced_Composite_Material_Portfolio_Selector_Guide.pdf (accessed: December 01, 2023).
- Product TC890. Available at: https://www.toraytac.com/product-explorer/products/mhdR/TC890 (accessed: July 07, 2023).
- High temperature composite materials. Available at: https://pdf4pro.com/amp/view/high-tempereture-composite-materials-upilex-5a5302.html (accessed: July 07, 2023).
- Zharinov M.A., Shimkin A.A., Akhmadieva K.R., Zelenina I.V., Valueva M.I. Melt polyimide binder grade VS-51 for heat-resistant PCM. III All-Rus. Scientific-technical Conf. “Polymer composite materials and production technologies of a new generation”. Moscow: VIAM, 2018, pp. 136–146.
- Valueva M.I., Zelenina I.V., Nacharkina A.V., Ahmadieva K.R. Technological features of obtaining high temperature polyimide carbons. Foreign experience (review). Trudy VIAM, 2022, no. 6 (112), paper no. 08. Available at: http://www.viam-works.ru (accessed: June 21, 2023). DOI: 10.18577/2307-6046-2022-0-6-80-95.
- Boychuk A.S., Dikov I.A., Chertishchev V.Yu., Generalov A.S. Determination of porosity in monolithic parts and assemblies of an aircraft wing, made of PCM, using the ultrasonic echo-pulse method. Defektoskopiya, 2019, no. 1, pp. 3–9.
- Dikov I.A., Boychuk A.S., Chertishchev V.Yu., Generalov A.S. Features of determining porosity in PCM parts using ultrasonic echo-pulse testing method. Main trends, directions and prospects for the development of non-destructive testing methods in the aerospace industry: materials X All-Rus. conf. “TestMat”. Moscow: VIAM, 2018, pp. 65–79.
