Methodological features of studying the water content in solid materials with closed porosity

Zaporozhskaya A.A., Marachovskiy P.C., Shorstov S.Yu.
UDC
550.4
DOI
10.18577/2307-6046-2024-0-1-92-100
Article PDF (Russian) (748.13 KB)
How to cite
Zaporozhskaya A.A., Marachovskiy P.C., Shorstov S.Yu. Methodological features of studying the water content in solid materials with closed porosity // Proceedings of VIAM. 2024. No. 1. DOI: 10.18577/2307-6046-2024-0-1-92-100. URL: https://test.viam.ru/en/journal/2024/1/9
Keywords
oil bearing rock, light hydrocarbons, porosity, core, petroleum fluids, water cut
Abstract

A method for the quantitative determination of water and qualitative content of hydrocarbons in oil-bearing rock is proposed using methods of simultaneous thermal analysis and gas chromatography with mass selective detection. A method for analyzing water and light hydrocarbons has been selected. A calibration characteristic was constructed to determine the quantitative water content. Samples of two rock types, namely, bituminous silicite and calcareous siliceous dolomite, were studied. There were developed dependencies of mass loss on temperature and time during gravimetric research. Using the results obtained, the water content in the oil-bearing rock was assessed. The error of the analysis method was calculated.

Reference list
  1. Denislamov I.Z., Gimaltdinov I.K., Denislamova A.I., Maksutov Z.A. Technological solutions for assessing the water cut of oil production wells. Izvestiya Tomskogo politekhnicheskogo universiteta. Inzhiniring georesursov, 2019, no. 9, pp. 60–69. DOI: 10.18799/24131830/2019/9/2256.
  2. Shcherbakova K.O. Analysis of the problem of high water cut in the production of horizontal wells. Izvestiya vysshikh uchebnykh zavedeniy. Geologiya i razvedka, 2022, no. 6, pp. 29–38. DOI: 10.32454/0016-7762-2022-64-6-29-38.
  3. Merkulova Yu.I., Kuznetsova V.A., Kodachenko E.N., Zheleznyak V.G. Study of the influence of the primer layer’s chemical nature on the properties of the coating system based on fluoropolyurethane enamel. Aviation materials and technologies, 2022, no. 1 (66), paper no. 09. Available at: http://www.journal.viam.ru (ассеssed: September 13, 2023). DOI: 10.18577/2713-0193-2022-0-1-110-119.
  4. Rodkina I.A., Kazak E.S. Quantitative determination of bound water in rocks of the Bazhenov Formation. Vestnik Moskovskogo universiteta. Geologiya, 2019, no. 4, pp. 34–44. DOI: 10.33623/0579-9406-2019-4-34-44.
  5. Konovalova L.N., Zinovyeva L.M., Gukasyan T.K. Reservoir physics: textbook. Stavropol: Publ. house of North Caucasian Federal Univ., 2016, 120 p.
  6. Ivanov M.K., Burlin Yu.K., Kalmykov G.A., Karnyushina E.E., Korobova N.I. Petrophysical methods for studying core material (Terrigenous sediments). Moscow: Publ. house of Moscow Univ., 2008, 112 p.
  7. Erofeev V.T., Salnikova A.I., Kablov E.N., Startsev O.V., Varchenko E.A. Study of the durability of bitumen composites under conditions of variable humidity, ultraviolet irradiation and sea water. Fundamentalnye issledovaniya, 2014, no. 12–12, pp. 2549–2556.
  8. Gimatudinov Sh.K., Shirkovsky A.I. Physics of oil and gas reservoirs. Moscow: Nedra, 1982, 311 p.
  9. Тabarin V.A., Demyantseva S.D. Determination of bound water content in cores using microwaves. Neftegazovoye delo, 2009, no. 1, pp. 1–28.
  10. Tabarin V.A., Pototsky A.Yu. Determination of bound water content in cores at ultrahigh frequencies. Vestnik Tyumenskogo gosudarstvennogo universiteta, 2014, no. 7, pp. 51–57.
  11. Andreeva R.Yu. Comparison of capillary pressure values obtained by centrifugation and capillarimetry methods. Ufimskiy Gosudarstvennyy Neftyanoy Tekhnicheskiy Universitet, 2016, no. 2 (3), pp. 1–3.
  12. Method for determining the content of bound water in oils and petroleum products: pat. 2044307 Rus. Federation; appl. 02.03.93; publ. 20.09.95.
  13. Method for determining bound water in minerals: pat. 1229662 Rus. Federation; appl. 22.05.84; publ. 07.05.86.
  14. Barinov D.Ya., Shorstov S.Yu., Razmahov M.G., Gulyaev A.I. Examination of thermophysical characteristics of a heat-protective material based on fiberglass during destruction. Aviation materials and technologies, 2021, no. 4 (65), paper no. 10. Available at: http://www.journal.viam.ru (accessed: September 13, 2023). DOI: 10.18577/2713-0193-2021-0-4-91-97.
  15. Karachevtsev F.N., Dvoretskov R.M., Zagvozdkina T.N. Determination of silver in aluminum alloys by atomic emission spectrometry with inductively coupled plasma. Aviation materials and technologies, 2022, no. 1 (66), paper no. 12. Available at: http://www.journal.viam.ru (accessed: September 13, 2023). DOI: 10.18577/2713-0193-2022-0-1-143-152.
  16. Kablov E.N., Grashhenkov D.V., Uvarova N.E. Researches by method of infrared spectroscopy of structural changes of gels in heat treatment process when receiving high-temperature glassceramic materials on technology sol-gel. Aviacionnye materialy i tekhnologii, 2011, no. 2, pp. 22–25.
  17. Karachevtsev F.N., Letov A.F., Slavin A.V. Uncertainty of the measurements results of the chemical composition and its methods assessment. Trudy VIAM, 2021, no. 8 (102), paper no. 10. Available at: http://www.viam-works.ru (accessed: September 13, 2023). DOI: 10.18577/2307-6046-2021-0-8-84-91.