Research of the scanning electron microscopy method deformation of microphase structure of polymeric matrix at mechanical loading
The scanning electron microscopy method (SEM) by special technique of high reso-lution has investigates deformation of microphase structure of surface fracture of poly-meric matrix in epoxy carbon-, glass- and organoplastics at mechanical loading. It is shown that under the influence of mechanical loading of composite there is reorganiza-tion of structure of matrix. It is revealed that thermosetting polymeric matrix in the course of mechanical loading are capable (is plastically irreversible) to be deformed up to partial or complete disintegration assotsiats particles of disperse phase with formation of structures of linear type. It is shown that of surface fracture epoxy carbon-, glass- and organoplastics at mechanical loading is defined by the deformation processes of «torsionny» (rotational) type connected with mutual turn of local volumes of matrix (torsions).
- Kablov E.N. Strategicheskie napravlenija razvitija materialov i tehnologij ih pererabotki na period do 2030 goda [Strategic directions of development of materials and technologies to process them for the period up to 2030] //Aviacionnye materialy i tehnologii. 2012. №S. S. 7–17.
- Istorija aviacionnogo materialovedenija. VIAM – 80 let: gody i ljudi [History of aviation materials. VIAM - 80 years: the years and people] /Pod obshh. red. akad. RAN, prof. E.N. Kablova. M.: VIAM. 2012. 520 s.
- Kirillov V.N., Starcev O.V., Efimov V.A. Klimaticheskaja stojkost' i povrezhdaemost' polimernyh kompozicionnyh materialov, problemy i puti reshenija [Climatic resistance and defectiveness of polymeric composite materials, problems and solutions] //Aviacionnye materialy i tehnologii. 2012. №S. S. 412–423.
- Murashov V.V. Opredelenie fiziko-mehanicheskih harakteristik i sostava polimernyh kompozicionnyh materialov akusticheskimi metodami [Determination of physical and mechanical properties and composition of the polymer composite materials by acoustic methods] //Aviacionnye materialy i tehnologii. 2012. №S. S. 465–475.
- Postnov V.I., Nikitin K.E., Burhan O.L., Petuhov V.I., Orzaev V.G. Issledovanie ul'trazvukovym metodom strukturnyh izmenenij v PKM v processe formovanija polimernyh kompozicionnyh materialov [Study of the ultrasonic method of structural changes in the RMB during the molding of polymeric composite materials] //Aviacionnye materialy i tehnologii. 2009. №3. S. 25–29.
- Deev I.S., Kobec L.P. Mikrostruktura jepoksidnyh matric [Microstructure epoxy matrix] //Mehanika kompozitnyh materialov.1986. №1. S. 3–8.
- Deev I.S., Kobec L.P. Fraktografija jepoksidnyh polimerov [Fractography epoxy resins] //Vysokomolekuljarnye soedinenija. Ser. A. 1996. T. 38. №4. S. 627–633.
- Deev I.S., Kobec L.P. Issledovanie mikrostruktury i mikropolej deformacij v polimernyh kompozitah metodom rastrovoj jelektronnoj mikroskopii [The microstructure and deformation microscopic fields in polymer composites by scanning electron microscopy] //Zavodskaja laboratorija. Diagnostika materialov. 1999. T. 65. №4. S. 27–34.
- Deev I.S., Kobec L.P. Strukturoobrazovanie v napolnennyh termoreaktivnyh polimerah [Pattern formation in filled thermosetting polymers] //Kolloidnyj zhurnal. 1999. T. 61. №5. S. 650–660.
- Kobec L.P., Deev I.S. Strukturoobrazovanie v termoreaktivnyh svjazujushhih i matricah kompozicionnyh materialov na ih osnove [Gelation in thermosetting binders and matrices of composite materials based on them] //Rossijskij himicheskij zhurnal. 2010. T. LIV. №1. S. 67–78.
- Mehanika razrushenija. Razrushenie materialov [Fracture mechanics. Fracture of Materials]: Per. s angl. /Pod red. R.V. Gol'-dshtejna. M.: Mir. 1979. 240 s.
- Kablov E.N., Deev I.S., Efimov V.A., Kavun N.S., Kobec L.P., Nikishin E.F. Vlijanie atmosfernyh faktorov i mehanicheskih naprjazhenij na mikrostrukturnye osobennosti razrushenija polimernyh kompozicionnyh materialov [Influence of weather conditions and mechanical stresses on the microstructural features of destruction of polymer composite materials] /V sb. dokl. VII nauch. konf. po gidroaviacii «Gidroaviasalon–2008». Ch. 1. M. 2008. S. 279–286.
- Gul' V.E. Struktura i prochnost' polimerov [The structure and strength of the polymer]. M.: Himija. 1971. 334 s.
- Narisava I. Prochnost' polimernyh materialov [Durability of polymeric materials]. M.: Himija. 1987. 400 s.
- Kobets L.P., Deev I.S. Carbon fibres: structure and mechanical properties //Composites Science and Technology. 1997. V. 57. P. 1571–1580.
- Litvinov V.B., Kobec L.P., Toksanbaev M.S., Deev I.S., Buchnev L.M. Strukturno-mehanicheskie svojstva vysokoprochnyh uglerodnyh volokon [Structural and mechanical properties of high carbon fibers] //Kompozity i nanostruktury. 2011. №3. S. 36–50.
- Deev I.S., Morgulec S.V., Shan'gina M.N. Issledovanie osobennostej stroenija i naprjazhenno-deformirovannogo sostojanija uglerodnyh volokon s razlichnoj formoj poperechnogo sechenija [The study of the structure and features of the stress-strain state of carbon fibers with different cross-sectional shape] //Materialovedenie. 2011. №1. S. 23–28.
- Deev I.S., Kobec L.P. Issledovanie mikrostruktury i osobennostej razrushenija jepoksidnyh polimerov i kompozicionnyh materialov na ih osnove. Ch. 1 [The micro-structure and fracture features of epoxy polymers and composite materials based on them. Part 1] //Materialovedenie. 2010. №5. S. 8–16.
- Deev I.S., Kobec L.P. Issledovanie mikrostruktury i osobennostej razrushenija jepoksidnyh polimerov i kompozicionnyh materialov na ih osnove. Ch. 2 [The micro-structure and fracture features of epoxy polymers and composite materials based on them. Part 2] //Materialovedenie. 2010. №6. S. 13–18.
- Deev I.S., Kobec L.P. «Torsionnoe» razrushenie jepoksidnyh polimerov i matric v polimernyh kompozicionnyh materialah [«Torsion» destruction of epoxy polymers and polymeric matrices in composite materials] /V sb. materialov IV Mezhdunarodnoj konf. «Deformacija i razrushenie materialov i nanomaterialov». M.: IMET RAN. 2011. S. 596–597.
- Deev I.S., Kobec L.P., Rumjancev A.F. Fraktograficheskie issledovanija jepoksidnyh ugleplastikov posle ispytanij na treshhinostojkost' po mode I [Fractographic studies of epoxy carbon fiber after crack resistance tests in the fashion I] //Kompozity i nanos-truktury. 2013. №2. S. 2–12.
- Deev I.S., Kobec L.P., Rumjancev A.F. Issledovanie osobennostej ustalostnogo rassloenija ugleplastikov v uslovijah otryva i sdviga [Investigation of the features of fatigue in carbon fiber bundle separation and shear conditions] /V sb. materialov V Mezhdunarodnoj konf. «Deformacija i razrushenie materialov i nanomaterialov». M.: IMET RAN. 2013. S. 585–587.
- Kitaeva N.S., Muhanova E.E., Deev I.S. Vysokoteplostojkie gidrofobnye pokrytija dlja teplozashhitnogo materiala na osnove kvarcevogo volokna [Vysokoteplostoykie hydro-phobic coatings for thermal barrier material based on silica fiber] //Trudy VIAM. 2013. №6. St. 03 (viam-works.ru).
- Larionov S.A., Deev I.S., Petrova G.N., Bejder Je.Ja. Vlijanie uglerodnyh napolnitelej na jelektrofizicheskie, mehanicheskie i reologicheskie svojstva polijetilena [Influence of carbon fillers on the electrical, mechanical and rheological properties of polyethylene] //Trudy VIAM. 2013. №9. St. 04 (viam-works.ru).
- Deev I.S., Belov P.A., Kobec L.P. Deformacionnaja anizotropija fazovoj mikrostruktury polimernyh matric pri silovom vozdejstvii [Deformation anisotropy phase microstructure of polymeric matrices by force action] /V sb. tezisov dokl. VI Vse-rossijskoj Karginskoj konf. «Polimery–2014». T. 1. M. 2014. S. 261.
- Korhov V.P., Fajtel'son E.A., Molchanov Ju.M. Uporjadochenie jepoksidnogo polimera pri orientirovanii [Streamlining the epoxy resin in the orientation] //Mehanika kompozitnyh materialov.1989. №6. S. 1103–1108.
- Deev I.S., Martynov A.M., Pasmor I.V., Aleksashin V.M., Gavrilov I.K. Vlijanie vysokih davlenij na strukturoobrazovanie jepoksidnyh oligomerov [Effect of high pressures on structure of epoxy oligomers] /V sb. tezisov dokl. IV Vsesojuznoj konf. po himii i fiziko-himii oligomerov. Chernogolovka. 1990. S. 115.
- Il'chenko S.I., Gunjaev G.M., Rumjancev A.F., Deev I.S., Aleksashin V.M. Izostaticheskoe formovanie polimernyh kompozicionnyh materialov [Isostatic molding of polymeric composite materials] /V sb. Aviacionnye materialy i tehnologii. Vyp. «Polimernye kompozicionnye materialy». M.: VIAM. 2002. S. 40–44.
