The phase composition researching of the diffusion layer of heat-resistant steel VKS10-U-Sh

Dvoretskov R.M., Kurpyakova N.A., Kolmykova N.A., Karachevtsev F.N.
UDC
669.14
DOI
10.18577/2307-6046-2015-0-10-5-5
Article PDF (Russian) (1010.19 KB)
How to cite
Dvoretskov R.M., Kurpyakova N.A., Kolmykova N.A., Karachevtsev F.N. The phase composition researching of the diffusion layer of heat-resistant steel VKS10-U-Sh // Proceedings of VIAM. 2015. No. 10. DOI: 10.18577/2307-6046-2015-0-10-5-5. URL: https://test.viam.ru/en/journal/2015/10/5
Abstract

The phase composition of the diffusion layer of high-strength heat-resistant precipitation-hardening steel VKS10-U-Sh, microalloyed with rare-earth metals (REM) after a comprehensive chemical and heat treatment, comprising the steps of vacuum carburizing, strengthening heat treatment (tempering, quenching, maraging and ion-plasma nitriding) has been investigated. The methods of physical-chemical phase analysis (PCPA), electron back scatter diffraction (EBSD) and scanning electron microscopy (SEM) have been used. The data obtained by different methods have allowed finding out which alloying elements form the phase composition of steel and which carbides and nitrides give it the necessary properties.

Reference list
  1. Kablov E.N. Innovacionnye razrabotki FGUP «VIAM» GNC RF po realizacii «Strategicheskih napravlenij razvitija materialov i tehnologij ih pererabotki na period do 2030 goda» [Innovative development of VIAM Federal State Unitary Enterprise of GNTs Russian Federation on implementation «The strategic directions of development of materials and technologies of their processing for the period till 2030»] //Aviacionnye materialy i tehnologii. 2015. №1 (34). S. 3–33.
  2. Kablov E.N., Ospennikova O.G., Vershkov A.V. Redkie metally i redkozemel'nye jele-menty – materialy sovremennyh i budushhih vysokih tehnologij [Rare metals and rare earth elements – materials of modern and future high technologies] //Trudy VIAM. 2013. №2. St. 01 (viam-works.ru).
  3. Gerasimov S.A., Kuksenova L.I., Lapteva V.G. Struktura i iznosostojkost' azotirovannyh stalej i splavov [Structure and wear resistance nitrated staly and alloys]. M.: MGTU im. N.Je. Baumana. 2012. 518 s.
  4. Gerasimov S.A., Kuksenova L.I., Lapteva V.G., Fahurtdinov R.S., Alekseeva M.S., Hrennikova I.A., Borejko N.L., Smirnov A.E., Krasovskij D.S. Vlijanie ionno-plazmennogo azotirovanija i vakuumnoj cementacii na iznosostojkost' stalej VKS-7 i VKS-10 [Influence of ion plasma nitriding and vacuum cementation on wear resistance staly VKS-7 and VKS-10] //Nauka i obrazovanie. 2013. №6. S. 391–400.
  5. Voznesenskaja N.M., Kablov E.N., Petrakov A.F., Shal'kevich A.B. Vysokoprochnye kor-rozionnostojkie stali austenitno-martensitnogo klassa [High-strength corrosion-resistant steel of the austenitno-martensitic class] //MiTOM. 2002. №7. S. 34–37.
  6. Mubojadzhjan S.A., Lucenko A.N., Aleksandrov D.A., Gorlov D.S. Issledovanie vozmozhnosti povyshenija sluzhebnyh harakteristik lopatok kompressora GTD metodom ionnogo modificirovanija poverhnosti [Research of possibility of increase of office characteristics of compressor blades of GTD by method of ionic modifying of surface] //Trudy VIAM. 2013. №1. St. 02 (viam-works.ru).
  7. Shherbakov A.I., Krylov S.A., Kalicev V.A., Ignatov V.A. Razrabotka tehnologii vyplavki vysokoprochnoj martensitostarejushhej stali VKS-180-ID (01N18K9M5T), mikrolegirovannoj RZM [Development of smelting technology of high-strength maraging steel VKS-180-ID (01Н18К9М5Т), microalloyed RZM] //Trudy VIAM. 2015. №2. St. 04 (viam-works.ru).
  8. Razuvaev E.I., Kapitanenko D.V. Vlijanie termomehanicheskoj obrabotki na strukturu i svojstva austenitnyh stalej [Influence of thermomechanical processing on structure and property austenitny staly] //Trudy VIAM. 2013. №5. St. 01 (viam-works.ru).
  9. Gromov V.I., Kurpjakova N.A., Sedov O.V., Korobova E.N. Vakuumnaja i ionno-plazmennaja himiko-termicheskaja obrabotka otvetstvennyh detalej gazoturbinnyh dvigatelej [Vacuum and ion-plasma chemical and thermal processing of responsible details of gas turbine engines] //Aviacionnye materialy i tehnologii. 2012. №S. S. 147–156.
  10. Tonysheva O.A., Voznesenskaja N.M., Shal'kevich A.B., Petrakov A.F. Issledovanie vlijanija vysokotemperaturnoj termomehanicheskoj obrabotki na strukturu, tehnologicheskie, mehanicheskie i korrozionnye svojstva vysokoprochnoj korrozionnostojkoj stali perehodnogo klassa s povyshennym soderzhaniem azota [Research of influence of high-temperature thermomechanical processing on structure, technological, mechanical and corrosion properties of high-strength corrosion-resistant steel of transitional class with the raised content of nitrogen] //Aviacionnye materialy i tehnologii. 2012. №3. S. 31–36.
  11. Gromov V.I., Utkina A.N., Kurpjakova N.A. Dispersionnoe tverdenie cementirovannogo sloja teplostojkih stalej martensitnogo klassa pri termicheskoj obrabotke [Dispersion hardening of tsementirovanny layer heatresistant staly the martensitic class at thermal processing] //Vestnik MGTU im. N.Je. Baumana. Ser. «Mashinostroenie». 2011. №SP2. S. 137–142.
  12. Tonysheva O.A., Voznesenskaja I.M., Eliseev Je.A., Shal'kevich A.B. Novaja vysokoprochnaja jekonomnolegirovannaja azotosoderzhashhaja stal' povyshennoj nadezhnosti [New high-strength ekonomnolegirovanny nitrogen-bearing steel of increased reliability] //Aviacionnye materialy i tehnologii. 2012. №S. S. 84–88.
  13. Gerasimov S.A., Kuksenova L.I., Lapteva V.G., Fahurtdinov R.S., Smirnov A.E., Gromov V.I., Stupnikov V.V. Issledovanie iznosostojkosti stalej VKS-7 i VKS-10 posle vakuumnoj cementacii i vakuumnoj nitrocementacii [Research of wear resistance staly VKS-7 and VKS-10 after vacuum cementation and vacuum nitrocementation] //Nauka i obrazovanie. 2013. №5. 345 s.
  14. Tarasenko L.V., Titov V.I., Utkina A.N. Svojstva i fazovyj sostav vysokouglerodistoj stali dlja zubchatyh koles aviacionnoj tehniki [Properties and phase composition of high-carbon steel for toothed wheels of aviation engineering] //Metallurgija mashinostroenija. 2012. №3. S. 10–14.
  15. Kablov E.N., Krivonogov G.S. Legirovanie i fazovaja nestabil'nost' vysokoprochnyh korrozionnostojkih stalej [Alloying and phase instability high-strength corrosion-resistant staly] //Metally. 2002. №2. S. 65–73.
  16. Lahtin Ju.M., Kogan Ja.D. Azotirovanie stali [Steel nitriding]. M.: Mashinostroenie. 1976. 15 s.
  17. Semenov M.Ju., Smirnov A.E., Lashnev M.M., Stupnikov V.V. Matematicheskaja model' vakuumnoj nitrocementacii teplostojkoj stali VKS-10 [Mathematical model of vacuum nitrocementation of VKS-10 heat-resistant steel] //Nauka i obrazovanie. 2013. №8. S. 76.
  18. Golubcova R.B. Fazovyj analiz nikelevyh splavov [Phase analysis of nickel alloys]. M.: Nauka. 1969. C. 5–33.
  19. Renata Chylinska, Malgorzata Garbiak, Bogdan Piekarski Electrolytic Phase Extraction in Stabilised Austenitic Cast Steel //Material Science (MEDŽIAGOTYRA). 2005. V. 11. №4. P. 348–351.
  20. Hye-Youn Lee, Masahiko Demura, Ya Xub, Dang-Moon Weea, Toshiyuki Hirano Selective dissolution of the γ phase in a binary Ni(γ)/Ni3Al(γ/) two-phase alloy //Corrosion Science. 2010. V. 52. P. 3820–3825.
  21. Lashko N.F., Zaslavskaja L.V., Kozlova M.N., Morozova G.I., Sorokina K.P., Jakovleva E.F. Fiziko-himicheskij analiz stalej i splavov [Physical and chemical analysis staly and alloys]. 2-e izd. M.: Metallurgija. 1978. 28 c.
  22. Lashko N.F., Zaslavskaja L.V., Kozlova M.N., Morozova G.I., Sorokina K.P., Hahlova N.V., Jakovleva E.F. Fiziko-himicheskie metody fazovogo analiza stalej i splavov [Physical and chemical methods of the phase analysis staly and alloys]. M.: Metallurgija. 1970. S. 9–19.
  23. Morozova G.I. K istorii sozdanija metoda fiziko-himicheskogo fazovogo analiza [To history of creation of method of the physical and chemical phase analysis] //MiTOM. 2006. №8. S. 19–21.
  24. Metod difrakcii otrazhennyh jelektronov v materialovedenii [Method of diffraction of the reflected electrons in materials science] /Pod red. A. Shvarca, M. Kumara, B. Adamsa, D. Filda. M.: Tehnosfera. 2014. 21 s.
  25. Danilenko V.N., Mironov S.Ju., Beljakov A.N., Zhiljaev A.P. Primenenie EBSD analiza v fizicheskom materialovedenii (obzor) [Application of EBSD of the analysis in physical materials science (review)] //Zavodskaja laboratorija. Diagnostika materialov. 2012. T. 78. №2. S. 28–46.
  26. Lashko N.F., Zaslavskaja L.V., Kozlova M.N., Morozova G.I., Sorokina K.P., Jakovleva E.F. Fiziko-himicheskij analiz stalej i splavov [Physical and chemical analysis staly and alloys]. 2-e. izd. M.: Metallurgija. 1978. C. 113–117.