Organosilicon polymer compounds based inorganic fibers for high-temperature composite materials (review)

Shestakov A.M., Khaskov M.A., Sorokin O.Ju.
Shestakov A.M., Khaskov M.A., Sorokin O.Ju. Organosilicon polymer compounds based inorganic fibers for high-temperature composite materials (review) // Proceedings of VIAM. 2019. No. 1. DOI: 10.18577/2307-6046-2019-0-1-74-91. URL: https://test.viam.ru/en/journal/2019/1/9
Keywords
silicon carbide, inorganic fibers, organosilicon polymer compounds, polycarbosilane, polysilazane, thermal-oxidative stability, phase composition, physical and mechanical properties.
Abstract

This article discusses the main types of organosilicon polymer compounds based inorganic fibers, produced abroad, for high-temperature composite materials of various nature. The methods for producing organosilicon polymer compounds and fibers are briefly described. Also, the effect of the nature of the organosilicon polymer and the method of producing fibers on their physical and mechanical properties, phase composition and thermal-oxidative stability is shown. The prospects for the use of fibers as reinforcing filler for high-temperature composites are shown.

Reference list
  1. Kablov E.N. Kompozity: segodnya i zavtra [Composites: today and tomorrow] // Metally Evrazii. 2015. №1. S. 36–39.
  2. Kablov E.N. Innovacionnye razrabotki FGUP «VIAM» GNC RF po realizacii «Strategicheskih napravlenij razvitiya materialov i tehnologij ih pererabotki na period do 2030 goda» [Innovative developments of FSUE «VIAM» SSC of RF on realization of «Strategic directions of the development of materials and technologies of their processing for the period until 2030»] // Aviacionnye materialy i tehnologii. 2015. №1 (34). S. 3–33. DOI: 10.18577/2071-9140-2015-0-1-3-33.
  3. Grashchenkov D.V. Strategiya razvitiya nemetallicheskih materialov, metallicheskih kompozicionnyh materialov i teplozashhity [Strategy of development of non-metallic materials, metal composite materials and heat-shielding] // Aviacionnye materialy i tehnologii. 2017. №S. S. 264–271. DOI: 10.18577/2071-9140-2017-0-S-264-271.
  4. Grashchenkov D.V., Evdokimov S.A., Zhestkov B.E., Solntsev S.St., Shtapov V.V. Issledovaniye termokhimicheskogo vozdeystviya potoka vozdushnoy plazmy na vysokotemperaturnyy keramicheskiy kompozitsionnyy material [Research of thermochemical influence of the air plasma flow on high-temperature ceramic composite material] // Aviacionnye materialy i tehnologii. 2017. №2 (47). S. 31–40. DOI: 10.18577/2071-9140-2017-0-2-31-40.
  5. Kablov E.N., Nikiforov A.A., Demin S.A., Chesnokov D.V., Vinogradov S.S. Perspektivnyye pokrytiya dlya zashchity ot korrozii uglerodistykh staley [Perspective coatings for corrosion protection of carbon steels] // Stal. 2016. №6. S. 70–81.
  6. Grashchenkov D.V., Efimochkin I.Yu., Bolshakova A.N. Vysokotemperaturnye metallomatrichnye kompozicionnye materialy, armirovannye chasticami i voloknami tugoplavkih soedinenij [High-temperature metal-matrix composite materials reinforced with particles and fibers of refractory compounds] // Aviacionnye materialy i tehnologii. 2017. №S. S. 318–328. DOI: 10.18577/2071-9140-2017-0-S-318-328.
  7. Kablov E.N., Grashchenkov D.V., Shchegoleva N.E., Orlova L.A., Suzdaltsev E.I. Radioprozrachnaya steklokeramika na osnove strontsiyalyumosilikatnogo stekla [Radiotransparent glass ceramics based on strontium-aluminosilicate glass] // Ogneupory i tekhnicheskaya keramika. 2016. №6. S. 31–37.
  8. Sorokin O.Yu. K voprosu o mehanizme vzaimodejstviya uglerodnyh materialov s kremniem (obzor) [On the issue of the mechanism of interaction between carbon materials and Si melt (review)] // Aviacionnye materialy i tehnologii. 2015. №1. S. 65–70. DOI: 10.18577/2071-9140-2015-0-1-65-70.
  9. Kablov E.N., Shchetanov B.V., Grashhenkov D.V., Shavnev A.A., Nyafkin A.N. Metallomatrichnye kompozicionnye materialy na osnove Al–SiC [Metalmatrix composite materials on the basis of Al–SiC] // Aviacionnye materialy i tehnologii. 2012. №S. S. 373–380.
  10. Kablov E.N., Grashchenkov D.V., Isayeva N.V., Solntsev S.S., Sevastyanov V.G. Vysokotemperaturnyye konstruktsionnyye kompozitsionnyye materialy na osnove stekla i keramiki dlya perspektivnykh izdeliy aviatsionnoy tekhniki [High-temperature structural composite materials based on glass and ceramics for promising products of aviation technology] // Steklo i keramika. 2012. №4. S. 7–11.
  11. Kablov E.N., Shchetanov B.V., Ivahnenko Yu.A., Balinova Yu.A. Perspektivnye armiruyushhie vysokotemperaturnye volokna dlya metallicheskih i keramicheskih kompozicionnyh materialov [Perspective reinforcing high-temperature fibers for metal and ceramic composite materials] // Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2013. №2. St. 05. Available at: http://www.viam-works.ru (accessed: December 11, 2018).
  12. Sorokin O.Yu., Grashhenkov D.V., Solntsev S.St., Evdokimov S.A. Keramicheskie kompozicionnye materialy s vysokoj okislitelnoj stojkostyu dlya perspektivnyh letatelnyh apparatov (obzor) [Ceramic composite materials with high oxidation resistance for the novel aircrafts (review)] // Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2014. №6. St. 08. Available at: http://www.viam-works.ru (accessed: December 11, 2018). DOI: 10.18577/2307-6046-2014-0-6-8-8.
  13. Sidorov D.V., Shcherbakova G.I. Vysokotekhnologichnyye komponenty kompozitsionnykh materialov i spetsialnyye volokna dlya shirokogo spektra primeneniya [High-tech components of composite materials and special fibers for a wide range of applications] // Khimicheskaya tekhnologiya. 2016. T. 17. №4. S. 183–192.
  14. Ichikawa H. Polymer-Derived Ceramic Fibers // Annual Review of Materials Research. 2016. Vol. 46. P. 6.1–6.22.
  15. Fritz G., Grofe J. Carbosilanes // Advanced Inorganic Chemistry and Radiochemistry. 1965. Vol. 7. P. 349.
  16. Yajima S., Okamura K., Hayashi J. Continuous silicon carbide fiber of high tensile strength // Chemistry Letters. 1975. Vol. 9. P. 931–934.
  17. Bansal N.P., Lamon J. Ceramic Matrix Composites: Materials, Modeling and Technology. New York. Wiley & Sons, 2014. P. 217–220.
  18. Schilling C.L., Wesson J.P., Williams T.C. Polycarbosilane precursors for silicon carbide // American Ceramic Society Bulletin. 1983. Vol. 62. P. 912–915.
  19. Ishikawa T. Recent developments of the SiC fibers NICALON and its composites, including properties of the SiC fiber HI-NICALON for ultra-high temperature // Composites Science Technology. 1994. Vol. 51. P. 135–144.
  20. Kyushin S., Ichikawa K. Study on the detailed structure of poly(dimethylsilylene) // Organometallics. 2014. Vol. 33. P. 6298–6303.
  21. Okamura K. Preparation of Preceramics from Polysilane. Tokyo: CMC, 1985. 179 p.
  22. Ichikawa H., Machino F., Teranishi H., Ishikawa T. Oxidation reaction of polycarbosilane // Silicon-Based Polymer Science: A Comprehensive Resource. Washington, DC: American Chemical Society, 1990. P. 619–637.
  23. Simon G., Bunsell A.R. Mechanical and structural characterization of the Nicalon silicon carbide fibre // Journal of Materials Science. 1984. Vol. 19. P. 3649–3657.
  24. Wynne K.J., Rice R.W. Ceramics via polymer pyrolysis // Annual Reviews of Materials Science. 1984. Vol. 14. P. 325–334.
  25. Yajima S. Tensile strength of SiC fibers as a function of fiber diameter // Philosophical Transactions of the Royal Society A. 1980. Vol. 294. P. 419–425.
  26. Ichikawa H. Effect of curing conditions on mechanical properties of SiC fibre (Nicalon) // Journal of Materials Science Letters. 1987. Vol. 6. P. 420–422.
  27. Laffon C., Flank A.M., Lagarde P. et al. Study of Nicalon-based ceramic fibers and powders by XAFS spectrometry, X-ray diffractometry and some additional methods // Journal of Materials Science. 1989. Vol. 24. P. 1503–1512.
  28. Ishikawa T., Ichikawa H. Strength and structure of SiC fiber after exposure to high temperature // Proceedings of the Symposium on High Temperature Materials Chemistry. 1987. Vol. 4. P. 205–217.
  29. Mah T. Thermal stability of SiC fibres (Nicalon) // Journal of Materials Science. 1984. Vol. 19. P. 1191–1201.
  30. Pysher D.J. Strength of ceramic fibers at elevated temperatures // Journal of the American Ceramic Society. 1989. Vol. 72. No. 2. P. 284–288.
  31. Shimoo T., Hayatsu T., Narisawa M. et al. Mechanism of ceramization of electron-irradiation cured polycarbosilane fiber // Journal of the Ceramic Society of Japan. 1993. Vol. 101. No. 7. P. 809–813.
  32. Okamura K., Seguchi T. Application of radiation curing in the preparation of polycarbosilane-derived SiC fibers // Journal of Inorganic and Organometallic Polymers Chemistry. 1992. Vol. 2. No. 1. P. 171–179.
  33. Sugimoto M., Shimoo T., Okamura K., Seguchi T. Reaction mechanisms of silicon carbide fiber synthesis by heat treatment of polycarbosilane fibers cured by radiation. 1. Evolved gas analysis // Journal of the American Ceramic Society. 1995. Vol. 78. No. 4. P. 1013–1017.
  34. Bodet R., Bourrat X., Lamon J., Nslain R. Tensile creep behavior of a silicon carbide-based fibre with a low oxygen content // Journal of Materials Science. 1995. Vol. 30. P. 661–667.
  35. Chollon G., Bodet R., Pailler R., Bourrat X. Structure and thermal evolution of SiC-based fibers with low oxygen content // Ceramic Transactions. 1995. Vol. 58. P. 305–310.
  36. Berger M.H., Bunsell A.R. Microstructure and thermal-mechanical stability of a low-oxygen Nicalon fibre // Journal of Microscopy. 1995. Vol. 177. No. 3. P. 230–241.
  37. Takeda M., Saeki A., Sakamoto J. et al. Effect of hydrogen atmosphere on pyrolysis of cured polycarbosilane fibers // Journal of the American Ceramic Society. 2000. Vol. 83. No. 5. P. 1063–1069.
  38. Takeda T., Sakamoto J., Imai Y. et al. Properties of stoichiometric silicon carbide fiber derived from polycarbosilane // Ceramic Engineering and Science Proceedings. 1994. Vol. 15. No. 4. P. 133–141.
  39. Ichikawa H., Okamura K., Seguchi T. Oxygen-free ceramic fibers from organosilicon precursors and E-beam curing // Ceramic Transactions. 1995. Vol. 58. P. 63–74.
  40. Takeda M., Sakamoto J., Saeki A. et al. High performance silicon carbide fiber Hi-Nicalon for ceramic matrix composites // Ceramic Engineering and Science Proceedings. 1995. Vol. 16. No. 4–5. P. 37–44.
  41. Takeda M., Sakamoto J., Saeki A., Ichikawa H. Mechanical and structural analysis of silicon carbide fiber Hi-Nicalon Type S // Ceramic Engineering and Science Proceedings. 1996. Vol. 17. No. 4. P. 35–42.
  42. Takeda M., Urano A., Sakamoto J., Imai Y. Microstructure and oxidation behavior of silicon carbide fibers derived from polycarbosilane // Journal of the American Ceramic Society. 2000. Vol. 83. No. 5. P. 1171–1176.
  43. Toreki W., Sacks M.D. Polymer-derived silicon carbide fibers with low oxygen content and improved thermomechanical stability // Composites Science Technology. 1994. Vol. 51. P. 145–159.
  44. Sacks M.D., Morrone A.A., Scheiffele G.W., Saleem M. Characterization of polymer-derived silicon carbide fibers with low oxygen content, near-stoichiometric composition, and improved thermomechanical stability // Ceramic Engineering and Science Proceedings. 1995. Vol. 16. No. 4. P. 25–35.
  45. Lipowitz J., Rabe J.A., Zank G.A. Polycrystalline SiC fibers from organosilicon polymers // Ceramic Engineering and Science Proceedings. 1991. Vol. 12. No. 9–10. P. 1819–1831.
  46. Xu Y., Zangvil A., Lipowitz J. et al. Microstructure and microchemistry of polymer-derived crystalline SiC fibers // Journal of the American Ceramic Society. 1993. Vol. 76. No. 12. P. 3034–3040.
  47. Lipowitz J., Barnard T., Bujaski D. et al. Fine-diameter polycrystalline SiC fibers // Composites Science Technology. 1994. Vol. 51. P. 167–171.
  48. Lipowitz J., Rabe J.A., Orr L.D., Androl R.R. Polymer derived stoichiometric SiC fibers // Materials Research Society Symposium Proceedings. 1994. Vol. 350. P. 99–104.
  49. Lipowitz J., Rabe J.A., Ngyuen K.T., Orr L.D., Androl R.R. Structure and properties of polymer-derived stoichiometric SiC fiber // Ceramic Engineering and Science Proceedings. 1995. Vol. 16. No. 4. P. 55–62.
  50. Lipowitz J., Rabe J.A., Zangvil A., Xu Y. Structure and properties of SYLRAMIC silicon carbide fiber: a polycrystalline, stoichiometric β-SiC composition // Ceramic Engineering and Science Proceedings. 1997. Vol. 18. No. 3. P. 147–157.
  51. DiCarlo J.A., Yun H.M. Non-oxide (silicon carbide) fibers // Handbook of Ceramic Composites. Editor N.P. Bansal. Boston: Kluwer Academic Publishers. 2005. P. 33–52.
  52. Yamamura T., Ishikawa T., Shibuya M. et al. Development of a new continuous Si–Ti–C–O fiber using an organometallic polymer precursor // Journal of Materials Science. 1988. Vol. 23. P. 2589–2594.
  53. Ichikawa H. Silicon carbide fibers (organometallic pyrolysis) // Comprehensive Composite Materials. Oxford: Elsevier Science, 2000. Vol. 1. P. 126–145.
  54. Fischbach D.B., Lemoine P.M., Yen G.V. Mechanical properties and structure of a new commercial SiC-type fibers (Tyranno) // Journal of Materials Science. 1988. Vol. 23. P. 987–993.
  55. Yajima S., Hasegawa Y., Okamura K., Matsuzawa T. Development of high tensile strength silicon carbide fibers using organosilicon precursor // Nature. 1978. Vol. 273. P. 525–527.
  56. Kumagawa K., Yamaoka H., Shibuya M., Yamamura T. Thermal stability and chemical corrosion resistance of newly developed continuous Si–Zr–C–O Tyranno fiber // Ceramic Engineering and Science Proceedings. 1997. Vol. 18. No. 3. P. 113–118.
  57. Ishikawa T., Kohtoku Y., Kumagawa K. et al. High-strength alkali-resistant sintered SiC fiber stable to 2200°C // Nature. 1998. Vol. 391. No. 6669. P. 773–775.
  58. Parthasarathy T.A., Mah T.I., Folsom C.A., Katz A.P. Microstructure stability of Nicalon at 1000°C in air after exposure to salt (NaCl) water // Journal of the American Ceramic Society. 1995. Vol. 78. No. 7. P. 1992–1996.
  59. Legrow G.E., Lim T.F., Lipowitz J., Reaoch R.S. Ceramics from hydridopolysilazane // Journal of the American Ceramic Society Bulletin. 1987. Vol. 66. No. 2. P. 363–367.
  60. Silicon nitride-containing ceramics: pat. US 4535007; publ. 13.08.85.
  61. Hydrosilazane polymers from (R3Si)2NH and HSiCl3: pat. US 4540803; publ. 10.09.85.
  62. Cannady J.P. Silicon nitride-containing ceramic material prepared by pyrolysis hydrosilazane polymers from (R3Si)2NH and HSiCl3: pat. US 4543344; publ. 24.09.85.
  63. Sawyer L.C., Jameleson M., Brikowski D., Haider M.I. Strength, structure and fracture properties of ceramic fibers produced from polymeric precursors // Journal of the American Ceramic Society. 1987. Vol. 70. No. 11. P. 798–810.
  64. Bunsell A.R. Inorganic fibers for composite materials // Composites Science Technology. 1994. Vol. 51. P. 127–133.
  65. Isoda T. Preparation of silicon nitride fibers // Development of Organosilicon Polymer. Tokyo: CMC, 1989. P. 210–231.
  66. Grisaffe S.J. Reinforcements: the key to high performance composites materials // NASA Technical Memorandum. 1990. No. 103230.
  67. Introducing SiNC-1400X ceramic fiber // Brochure. MATECH. URL: http://www.matechgsm.com/brochures/SiNC1400X.pdf (дата обращения: 29.11.2018).
  68. Baldus H.P., Passing G., Scholz H. et al. Properties of amorphous SiBNC ceramic fibers // Key Engineering Materials. 1997. No. 127. P. 177–184.
  69. Baldus H.P., Passing G. Si–B–(N, C): a new ceramic material for high performance applications // Advanced Structural Fiber Composites. Faenza: Techna, 1995. P. 125–132.