Specificity of application of X-ray methods of «swing» and Laue in determining the quality of the structure of castings of nickel heat-resistant alloys
Systematically analyzes and justifies the characteristics of equipment operating in monochromatic radiation by the «swing» method and in polychromatic radiation by the Laue method in relation to the specifics of controlled samples in the technology of single-crystal casting from nickel heat-resistant alloys. The main application of the «swing» method is the mass control of seed blanks, seedings, growth cones of samples and blades. The main application of the Laue method is local measurements of block misorientation in the casting of the turbine blade, determination of the crystallographic orientation misorientation in controlled areas on the blade. An optimized configuration is proposed for a compact modification of a diffractometer operating in monochromatic radiation for mass control of the structure in production.
- Fetisov G.V. Synchrotron radiation. Methods for studying the structure of substances. Moscow: Fizmatlit, 2007, 672 p.
- Lisoyvan V.I., Zadneprovsky G.M. On the method of determining the orientation of the crystallographic plane in a single crystal on a diffractometer. Apparatura i metody rentgenovskogo analiza, 1969., is. 4, pp. 64–70.
- Heiker D.M. X-ray diffractometry of single crystals. Leningrad: Mashinostroenie, 1973, 256 p.
- Shamray V.F., Lifshits V.A., Serebryany V.N. and others. Experience of using the DRON-7 diffractometer with the PGTM attachment for the study of textures. Zavodskaya laboratoriya. Diagnostika materialov, 2009, vol. 75, no. 1, pp. 32–35.
- Nazarkin R.M., Kolodochkina V.G., Ospennikova O.G., Orlov. M.R. The microstructure modifications of single crystals of Ni-based superalloys in time-tested turbine blades. Aviacionnye materialy i tehnologii, 2016, no. 4 (45), pp. 9–17. DOI: 10.18577/2071-9140-2016-0-4-9-17.
- Nazarkin R.M. X-ray diffraction techniques for precise determination of lattice constants in Ni-based superalloys: a brief review. Aviacionnye materialy i tehnologii, 2015, no. 1 (34), pp. 41–48. DOI: 10.18577/2071-9140-2015-0-1-41-48.
- Goganov D.A., Kazansky B.V., Klimenskaya D.A. et al. Position-sensitive detectors of soft X-ray radiation and their application. Pribory i tekhnika eksperimenta, 2015, no. 1, pp. 109–116.
- Pyankova L.A., Elokhin V.A., Arkhipov S.N. et al. Control of functional layers of HTSC-2 using a texture attachment of an X-ray diffractometer "Difrey-401". Zavodskaya laboratoriya. Diagnostika materialov, 2016, no. 82 (10), pp. 44–46.
- Abyzov A.M. X-ray diffraction analysis of polycrystalline substances on a mini-diffractometer "Difrey": textbook. Saint Petersburg: SPbGTI (TU), 2008, 95 p.
- Nazarkin R.M. Small-sized x-ray diffractometers for structure and phase analysis purposes (review). Trudy VIAM, 2019, no. 9 (81), paper no. Available at: http://www.viam-works.ru (accessed: May 12, 2021). DOI: 10.18577/2307-6046-2019-0-9-89-99.
- Umansky M.M. X-ray structural research equipment. Moscow: Fizmatgiz, 1960.348 p.
- Sidokhin F.A., Sidokhin A.F., Sidokhin E.F. On the determination of the crystallographic orientation of single crystals by the Laue method. Zavodskaya laboratoriya. Diagnostika materialov, 2009, vol. 75, no. 1, pp. 35–37.
- Potrakhov N.N., Khayutin S.G., Lifshits V.A., Oses R. Installation PRDU-KROS for express determination of crystallographic orientation of cubic single crystals by inverse Lauegrams. Zavodskaya laboratoriya. Diagnostika materialov, 2015, vol. 81, no. 8, pp. 27–30.
- Kuzmina N.A., Lifshits V.A., Potrakhov E.N., Potrakhov N.N. Comparative structure control of single-crystal castings of nickel superalloys x-ray diffraction methods of oscillation and Laue. Trudy VIAM, 2019, no. 9 (81), paper no. 02. Available at: http://www.viam-works.ru (accessed: March 12, 2021). DOI: 10.18577/2307-6046-2019-0-9-15-25.
- Petrushin N.V., Ospennikova O.G., Svetlov I.L. Single-crystal Ni-based superalloys for turbine blades of advanced gas turbine engines. Aviacionnye materialy i tehnologii, 2017, no. S, pp. 72−103. DOI: 10.18577/2071-9140-2017-0-S-72-103.
- Kablov E.N., Sidorov V.V., Kablov D.E., Min P.G. The metallurgical fundamentals for high quality maintenance of single crystal heat-resistant nickel alloys. Aviacionnye materialy i tehnologii, 2017, no. S, pp. 55–71. DOI: 10.18577/2071-9140-2017-0-S-55-71.
- Toloraya V.N., Kablov E.N., Demonis I.M. Technology of obtaining single-crystal casts of GTE blades of a given crystallographic orientation from rhenium-containing heat-resistant alloys. The effect of S.T. Kishkina. Moscow: Nauka, 2006, pp. 206–219.
- Kablov E.N., Bondarenko Yu.A., Kablov D.E. Features of structure and heat resisting properties of monocrystals of 001> high-rhenium nickel hot strength alloys received in the conditions of high-gradient directed crystallization. Aviacionnye materialy i tehnologii, 2011, no. 4, pp. 25–31.
- Kablov E.N., Bondarenko Yu.A., Echin A.B. Investigation of the influence of variable controlled temperature gradient on structural features, phase composition, properties of high-temperature heat-resistant alloys during their directional crystallization. Vestnik MGTU im. N.E. Bauman, ser.: Mechanical engineering, 2016, no. 6 (111), pp. 43–61.
- Toloraya V.N., Kablov E.N., Svetlov I.L., Orekhov N.G., Golubovsky E.R. Anisotropy of strength characteristics of single crystals of heat-resistant nickel alloys. Gorny informatsionno-analiticheskiy byulleten, 2005, special issue, pp. 225–236.
- Toloraya V.N., Kablov E.N., Orekhov N.G., Ostroukhova G.A. Structure and growth defects of single crystals of heat-resistant nickel alloys. Gorny informatsionno-analiticheskiy byulleten, 2005, special issue, pp. 190–202.
- Sidokhin E.F., Sidokhin F.A., Khayutin S.G. On the substructure of monocrystalline GTE blades. Aviatsionnaya promyshlennost, 2009, no. 1, pp. 34–36.
- Macro- and microstructure of nickel heat-resistant alloys intended for monocrystalline casting of blades. Available at: https://studme.org/151298/tehnika/makro_mikrostruktura_nikelevyh_zharoprochnyh_splavov_prednaznachennyh_monokristalnogo_litya_lopatok (accessed: October 14, 2020).
- Petrushin N.V., Visik E.M., Elyutin E.S. Improvement of the chemical composition and structure of castable nickel-base superalloy with low density. Part 2. Trudy VIAM, 2021, no. 4 (98), paper no. 01. Available at: http://www.viam-works.ru (accessed: June 12, 2021). DOI: 10.18577/2307-6046-2021-0-4-3-15.
- Oses R.Kh., Lifshits V.A., Potrakhov E.N., Potrakhov N.N. Program for decoding inverse laue patterns of fcc single crystals to determine the crystallographic orientation of samples (CGO analysis): Certificate of State Registration Computer Program no. 2011614448 (dated: June 6, 2011).
