Methodological features of studying the density of metal powder compositions at high temperature

Shorstov S.Yu., Dmitriev N.S., Razmakhov M.G., Skuridina N.S.
UDC
669.018.44:669.245
DOI
10.18577/2307-6046-2024-0-8-111-120
Article PDF (Russian) (810.24 KB)
How to cite
Shorstov S.Yu., Dmitriev N.S., Razmakhov M.G., Skuridina N.S. Methodological features of studying the density of metal powder compositions at high temperature // Proceedings of VIAM. 2024. No. 8. DOI: 10.18577/2307-6046-2024-0-8-111-120. URL: https://test.viam.ru/en/journal/2024/8/10
Keywords
metal powder compositions, granulometric composition, heat-resistant nickel alloys, centrifugal spraying of cast blanks, temperature coefficient of linear expansion, thermophysical properties, bulk density, true density
Abstract

This paper proposes an approach to estimating the density of solid materials at elevated temperatures, based on measuring the temperature coefficient of linear expansion. Measurements of metal powder compositions of alloys EP741NP, VZh178P and VZh159 were carried out. The temperature dependences of the density of the powders under study were established in the temperature range from 200 to 1100 ºС and the correctness of the results obtained was assessed. The features of the experiment are shown, and the advantages and disadvantages of the proposed measurement method are considered.

Reference list
  1. Kablov E.N., Antipov V.V. The role of new generation materials in ensuring the technological sovereignty of the Russian Federation. Vestnik Rossiyskoy akademii nauk, 2023, vol. 93, no. 10, pp. 907–916.
  2. Kablov E.N. No future without new materials. Metallurg, 2013, no. 12, рp. 4–8.
  3. Kablov E.N., Bakradze M.M., Gromov V.I., Voznesenskaya N.M., Yakusheva N.A. New high strength structural and corrosion-resistant steels for aerospace equipment developed by FSUE «VIAM» (review). Aviacionnye materialy i tehnologii, 2020, no. 1 (58), pp. 3–11. DOI: 10.18577/2071-9140-2020-0-1-3-11.
  4. Garibov G.S., Vostrikov A.V., Grits N.M., Fedorenko E.A. Development of new granulated heat-resistant nickel alloys for the production of disks and shafts of aircraft engines. Tekhnologiya legkikh splavov, 2010, no. 2, pp. 34–44.
  5. Garibov G.S., Grits N.M. V.I. Dobatkin and metallurgy of granules of heat-resistant nickel alloys. Tekhnologiya legkikh splavov, 2015, no. 2, pp. 34–39.
  6. Loshchinin Yu.V., Pakhomkin S.I., Razmakhov M.G. Phase transformation temperatures and calorimetric analysis of powder compositions of nickel-based superalloys. Aviacionnye materialy i tehnologii, 2020, no. 1 (58), pp. 79–85. DOI: 10.18577/2071-9140-2020-0-1-79-85.
  7. Vostrikov A.V., Lomberg B.S., Letnikov M.N., Ovsepyan S.V. Modern heat-resistant deformable nickel alloys of VIAM for gas turbine engine parts. All-Rus. Sci. and Tech. Conf. «Modern heat-resistant deformable nickel alloys and technologies for their production». Moscow: NRC «Kurchatov Institute» – VIAM, 2021, pp. 5–14.
  8. Volkov A.M., Vostrikov A.V., Bakradze M.M. Development principles and alloying features of p/m Ni-base superalloys for jet-engine disks application. Trudy VIAM, 2016, no. 8, paper no. 2. Available at: http://www.viam-works.ru (accessed: March 06, 2024). DOI: 10.18577/2307-6046-2016-0-8-2-2.
  9. Sukhov D.I., Nerush S.V., Efimochkin I.Yu., Karachevchev F.N., Bogachev I.A. Production of MMC based on VZh159 alloy by selective laser melting. Aviation materials and technologies, 2021, no. 2 (63), paper no. 07. Available at: http://www.journal.viam.ru (accessed: March 06, 2024). DOI: 10.18577/2713-0193-2021-0-2-62-72.
  10. Movenko D.A., Shurtakov S.V. Microcrack formation and controlling in nickel superalloys processed by selective laser melting (review). Aviation materials and technologies, 2022, no. 2 (67), paper no. 04. Available at: http://www.journal.viam.ru (accessed: March 06, 2024). DOI: 10.18577/2713-0193-2022-0-2-43-51.
  11. Volkov A. M., Shestakova A. A., Bakradze M. M. The comparison of powder produced by gas atomization and by plasma rotate electrode process in the point of production disk billets from Ni-base superalloys. Trudy VIAM, 2018, no. 11 (71), paper no. 02. Available at: http://www.viam-works.ru (accessed: March 06, 2024). DOI: 10.18577/2307-6046-2018-0-11-12-19.
  12. Bakradze М.М., Volkov А.М., Shestakova А.А., Letnikov M.N., Bubnov M.V. The features of the grains size changing in the p/m Ni-base superalloy for disks application produced via different technologies. Trudy VIAM, 2018, no. 2, paper no. 01. Available at: http://www.viam-works.ru (accessed: March 06, 2024). DOI: 10.18577/2307-6046-2018-0-2-1-1.
  13. Koshelev V.Ya., Garibov G.S., Sukhov D.I. Basic regularities of the process of producing granules of heat-resistant alloys by plasma spraying of a rotating workpiece. Tekhnologiya legkikh splavov, 2015, no. 3, pp. 97–103.
  14. Sokolovsky S.S., Astapovich O.S. Selection of the method and means for measuring the density of porous composite materials with open pores. 12th Int. Sci. and Tech. Conf. «Instrument Engineering–2019». Minsk: Belarusian National Tech. Univ., 2019, pp. 228–229.
  15. Gainullin Ren.Kh., Gainullin Rish.Kh., Tsvetkova E.M. et al. Mathematical justification of the technological parameters of the device for measuring the apparent density of porous materials. Lesnoy vestnik, 2022, vol. 26, no. 4, pp. 128–134. DOI: 10.18698/2542-1468-2022-4-128-134.
  16. Gainullin Ren.Kh., Gainullin Rish. Kh., Tsvetkova E.M. et al. Method for measuring the volume and determining the density of porous materials. Sistemy. Metody. Tekhnologii, 2021, no. 2 (50), pp. 106–110. DOI: 10.18324/2077-5415-2021-2-106-110.
  17. Chaplygin V.Yu. Methodology for studying metal powders obtained by electrical discharge dispersion. Sovremennye materialy, tekhnika i tekhnologii, 2016, no. 1 (4), p. 225–231.
  18. State Standard R 52802–2007. Heat-resistant granulated nickel alloys. Brands. Moscow: Standartinform, 2008, 10 p.
  19. State Standard 5632–2014. Stainless steels and alloys, corrosion-resistant, heat-resistant and heat-resistant. Brands. Moscow: Standartinform, 2015, 57 p.
  20. Kablov E.N. Innovative developments of FSUE «VIAM» SSC of RF on realization of «Strategic directions of the development of materials and technologies of their processing for the period until 2030». Aviacionnye materialy i tehnologii, 2015, no. 1 (34), pp. 3–33. DOI: 10.18577/2071-9140-2015-0-1-3-33.