Slice testing of structural aviation materials and coatings

Erasov V.S., Sibayev I.G., Sutubalov A.I.
Erasov V.S., Sibayev I.G., Sutubalov A.I. Slice testing of structural aviation materials and coatings // Proceedings of VIAM. 2025. No. 3. DOI: 10.18577/2307-6046-2025-0-3-101-116. URL: https://test.viam.ru/en/journal/2025/3/9
Keywords
slice, sample, coating, deformation, stress, fracture, laminate, fiber, sclerometry
Abstract

The article provides an analysis of domestic and foreign methods of mechanical testing of structural aviation composite materials and coatings on a slice. The types of cross-section fittings and their main differences are presented. The development of testing methods by instrumental indentation and scratching (sclerometry) is shown, in which destruction occurs by cutting the material with an indenter. A typical slice diagram in the coordinates «load‒displacement of the punch», diagrams of embedding and scratching with indentors, photographs of scratches without destruction and with traces of destruction on the deformable surface are presented.

Reference list
  1. Lavrov A.V., Yerasov V.S., Dyachenko O.A. Comparative analysis of domestic and foreign methods of double shear testing of aviation bolts. Kommentarii k standartam, TU, sertifikatam: yezhemesyachnoye prilozheniye k zhurnalu «Vse materialy. Entsiklopedicheskiy spravochnik», 2013, no. 11, pp. 2–7.
  2. Erasov V.S., Oreshko E.I. Mechanical testing and properties of structural aircraft metal materials: a tutorial. Ed. E.N. Kablov. Moscow: NRC «Kurchatov Institute» – VIAM, 2023, 344 p.
  3. Methods of testing, monitoring and research of engineering materials: a reference in 3 vols. Ed. A.T. Tumanov. Moscow: Mashinostroenie, 1974, vol. II: Methods of studying mechanical properties of metals, pp. 45–49.
  4. Industry standard 1 31101‒80. Bolts, screws and studs. Specifications. Moscow, 1980, 28 p. Available at: https://standartgost.ru (accessed: July 16, 2024).
  5. Industry standard 1 00552‒72. Bolts, screws made of titanium alloy. Technical conditions. Moscow, 1972, 16 p. Available at: https://standartgost.ru (accessed: July 16, 2024).
  6. Industry standard 1 90148‒74. Metals. Shear Test Method. Moscow, 1975, 8 p. Available at: https://standartgost.ru (accessed: July 16, 2024).
  7. MIL-STD-1312/13A. Fastener Test Methods. Method 13. Double Shear Test. Department of Defense of the USA. Washington. 1997, 10 p.
  8. MIL-STD-1312-20. Fastener Test Method. Method 20. Single Shear. Aerospase Industries Association of America, Inc., 1997, 14 p.
  9. ASTM F606/F606M-2016. Standard Test Methods for Determining the Mechanical Properties of Externally and Internally Threaded Fasteners, Washers, Direct Tension Indicators, and Rivets. American Society for Testing and Materials, 2013, 19 p.
  10. ASTM B565-04. Standard Test Method for Shear Testing of Aluminum and Aluminum-Alloy Rivets and Cold-Heading Wire and Rods. American Society for Testing and Materials, 2015, 5 p.
  11. ASTM B831-19. Test Method for Shear Testing of Thin Aluminum Alloy Products. American Society for Testing and Materials, 2019, 5 p.
  12. State Standard R 57968‒2017. Polymer composites. Method for testing samples for shear. Moscow: Standartinform, 2018, 15 p.
  13. Device for testing plastics for shear: pat. RU 167675 U1 Russian Federation; appl. 04.08.16; publ. 10.01.17.
  14. ASTM D732-17. Standard Test Method for Shear Strength of Plastics by Punch Tool. American Society for Testing and Materials, 2010, 4 p.
  15. Konovalov V.V. Methodology for certification of structural metal materials of aircraft airframes. Trudy TSAGI, 2013, is. 2725, pp. 21–80.
  16. State Standard 21318–75. Microhardness measurement by scratching with diamond tips. Moscow: Publ. House of Standards, 1976, 30 p.
  17. Golovin Yu.I. Nanoindentation and mechanical properties of materials at the submicro- and nanoscale. Recent results and achievements (Review). Fizika tverdogo tela, 2021, vol. 63, is. 1, pp. 3–42. DOI: 10.21883/FTT.2021.01.50395.171.
  18. ISO 14577-1:2015. Metallic materials – Instrumented indentation test for hardness and materials parameters – Part 1: Test method. International Organization for Standardization, 2015, 54 p.
  19. ISO 14577-2:2015. Metallic materials ‒ Instrumented indentation test for hardness and materials parameters – Part 2: Verification and calibration of testing machines. International Organization for Standardization, 2015, 32 p.
  20. ISO 14577-3:2015. Metallic materials ‒ Instrumented indentation test for hardness and materials parameters ‒ Part 3: Calibration of reference blocks. International Organization for Standardization, 2015, 16 p.
  21. ISO 14577-4:2016. Metallic materials ‒ Instrumented indentation test for hardness and materials parameters – Part 4: Test method for metallic and non-metallic coatings. International Organization for Standardization, 2016, 26 p.
  22. ASTM D7027-20. Standard Test Method for Evaluation of Scratch Resistance of Polymeric Coatings and Plastics Using an Instrumented Scratch Machine. American Society for Testing and Materials, 2020, 9 p.
  23. ASTM E2546-15. Standard Practice for Instrumented Indentation Testing. American Society for Testing and Materials, 2023, 23 p.
  24. ASTM G171-03. Standard Test Method for Scratch Hardness of Materials Using a Diamond Stylus. American Society for Testing and Materials, 2017, 7 p.
  25. State Standard R 56232‒2014. Determination of the stress-strain diagram by the instrumental indentation of a ball. General requirements. Moscow: Standartinform, 2018, 41 p.
  26. State Standard R 8.748‒2011 (ISO 14577-1:2002). State system for ensuring the uniformity of measurements. Metals and alloys. Measurement of hardness and other characteristics of materials by instrumental indentation. Part 1. Test method. Moscow: Standartinform, 2018, 28 p.
  27. State Standard R 8.904‒2015. State system for ensuring the uniformity of measurements. Measurement of hardness and other characteristics of materials by instrumental indentation. Part 2. Verification and calibration of hardness testers. Moscow: Standartinform, 2018, 30 p.
  28. State Standard R 8.907–2015. State verification scheme for hardness measuring instruments according to the Martens and indentation scales. Moscow: Standartinform, 2018, 8 p.
  29. Marchenkov A.Yu., Terentyev E.V. Scale effect in scratch tests of materials with different deformable volumes. Zavodskaya laboratoriya. Diagnostika materialov, 2017, vol. 83, no. 9, pp. 66‒69.
  30. Brinkevich D.I., Prosolovich V.S., Yankovsky Yu.N. et al. Sclerometric method for measuring the microhardness of photoresist on silicon. Pribory i metody izmereniy, 2016, vol. 7, no. 1. 77–84. DOI: 10.21122/2220-9506-7-1-77-84.
  31. Lvova N.A., Kravchuk K.S., Shirokov I.A. Algorithms for processing scratch images in the sclerometry method. Fizika tverdogo tela, 2013, vol. 55, is. 8, pp. 1570–1577.
  32. Useinov A., Reshetov V., Maslenikov I., Kravchuk K. ISO is easy! Nanoindustriya, 2015, no. 7, pp. 52–60.
  33. Useinov S.S. Measuring the hardness of structural materials by indentation and sclerometry methods on the submicron and nanometer scales: thesis abstract, Cand. Sc. (Tech.). Moscow: FGU TISNUM, 2010, 27 p.
  34. Sutubalov A.I., Podzhivotov N.Yu., Shershak P.V., Yakovlev N.O. Evaluation of homogeneity of physical and mechanical properties of semi-finished products for aviation purpose. Aviation materials and technologies, 2024, no. 1 (74), paper no. 10. Available at: http://www.journal.viam.ru (accessed: July 17, 2024). DOI: 10.18577/2713-0193-2024-0-1-121-135.
  35. Erasov V.S., Sibayev I.G. Scheme for the development and evaluation of properties of structural aviation composite materials. Aviation materials and technologies, 2023, no. 1 (70), paper no. 05. Available at: http://www.journal.viam.ru (accessed: July 19, 2024). DOI: 10.18577/2713-0193-2023-0-1-61-81.
  36. EN 1071-3. Advanced technical ceramics – Methods of test for ceramic coating – Part 3: Determination of adhesion and other mechanical failure modes by scratch test. European committee for standardization, 2005, 11 p.
  37. ISO 20502-2005(E). Fine ceramics (advanced ceramics, advanced technical ceramics) – Determination of adhesion of ceramic coatings by scratch testing. International Organization for Standardization, 2005, 8 p.
  38. ISO 1518-1:2023(E). Paints and varnishes – Determination of scratch resistance – Part 1: Constant-loading method. International Organization for Standardization, 2005, 6 p.
  39. ASTM D7187-20. Standard Test Method for Measuring Mechanistic Aspects of Scratch/Mar Behavior of Paint Coatings by Nanoscratching. American Society for Testing and Materials, 2020, 12 p.
  40. ASTM C1624-22. Standard Test Method for Adhesion Strength and Mechanical Failure Modes of Ceramic Coatings by Quantitative Single Point Scratch Testing. American Society for Testing and Materials, 2022, 28 p.
  41. Snarsky A.S., Krylenko A.V. Determination of physical and mechanical characteristics of a material by non-destructive testing. Fundamentalnye nauki. Mekhanika, 2005, no. 10, pp. 133–137.
  42. Gogolinsky K.V., Syasko V.A. Methods and means for monitoring mechanical properties of micro- and nanometer coatings and modified surface layers. Available at: https://ntcexpert.ru/documents/
  43. metody-pokrytij.pdf?ysclid=lwkg18gy4p195748077 (accessed: July 19, 2024).
  44. Golovin Yu.I., Tyurin A.I. Nano- and microhardness of solids – modern problems. Vestnik TGU, 2000, vol. 5, is. 2–3, pp. 251–253.
  45. Berkovich E.S., Kraposhina L.B. New IMASH device – interference depth gauge – for testing microhardness by indentation depth. New in the field of microhardness testing. Moscow: Nauka, 1974, pp. 93–100.
  46. Oreshko E.I., Erasov V.S., Utkin D.A., Avtayeva Ya.V. The equipment for definition of physicomechanical characteristics of materials by press-in method (review). Aviation materials and technologies, 2021, no. 4 (65), paper no. 12. Available at: http://www.journal.viam.ru (accessed: July 19, 2024). DOI: 10.18577/2713-0193-2021-0-4-107-124.
  47. Oreshko E.I., Erasov V.S., Yakovlev N.O., Utkin D.A. Methods for determining the mechanical characteristics of materials using indentation (review). Aviation materials and technology, 2021, no. 1 (62), paper no. 10. Available at: http://www.journal.viam.ru (accessed: July 19, 2024). DOI: 10.18577/2713-0193-2021-0-1-104-118.
  48. Lapitskaya V.A., Kuznetsova T.A., Chizhik S.A., Grinchuk P.S. Determination of crack resistance using AFM. Reports XIII Int. Conf. «Methodological aspects of scanning probe microscopy». Minsk, 2018, pp. 260–266.
  49. Shershak P.V., Sutubalov A.I., Yakovlev N.O., Sherstyuk F.A. Standards test methods for polymer matrix composite materials. Part 2. Compression properties. Aviation materials and technologies, 2024, no. 2 (75), paper no. 12. Available at: http://www.journal.viam.ru (accessed: July 19, 2024). DOI: 10.18577/2713-0193-2024-0-2-149-166.
  50. Monakhov A.D., Gulyaev M.M., Gladysheva N.E., Kopteltseva O.Yu., Avtaev V.V., Yakovlev N.O., Gulina I.V. Application of the digital image correlation method for constructing deformation diagrams in true coordinates. Izvestiya vysshikh uchebnykh zavedeniy. Tsvetnaya metallurgiya, 2023, vol. 29, no. 3, рр. 79–88. DOI: 10.17073/0021-3438-2023-3-79-88.
  51. Anton Paar Scratch Testers. Available at: http://www.anton-paar.com (accessed: July 19, 2024).