Selective laser sintering of polymer compositions based on polyamide 12

Sorokin A.E., Platonov M.M., Larionov S.A.
UDC
678.073
DOI
10.18577/2307-6046-2017-0-9-5-5
Article PDF (Russian) (931.6 KB)
How to cite
Sorokin A.E., Platonov M.M., Larionov S.A. Selective laser sintering of polymer compositions based on polyamide 12 // Proceedings of VIAM. 2017. No. 9. DOI: 10.18577/2307-6046-2017-0-9-5-5. URL: https://test.viam.ru/en/journal/2017/9/5
Keywords
powder composition, polyamide 12, selective laser sintering, 3D printing, density, fractional composition, melting, crystallization.
Abstract

Studies of crystallization from solution and processing by selective laser alloying of polyamide 12 based compositions have been carried out. It has been shown that process of crystallization under conditions close to equilibrium in the presence of nanoscale silicon dioxide makes it possible to obtain powder compositions with an optimal complex of properties. It has been found that Powder compositions with a narrow particle size distribution (from 20 to 100 μm) and a bulk density of not less than 0,4 g/cm3 can be processed by selective laser sintering into homogeneous samples with a high degree of monolithicity.

Reference list
  1. Kablov E.N. Innovacionnye razrabotki FGUP «VIAM» GNC RF po realizacii «Strategicheskih napravlenij razvitiya materialov i tehnologij ih pererabotki na period do 2030 goda» [Innovative developments of FSUE «VIAM» SSC of RF on realization of «Strategic directions of the develop-ment of materials and technologies of their processing for the period until 2030»] //Aviacionnye materialy i tehnologii. 2015. №1 (34). S. 3–33. DOI: 10.18577/2071-9140-2015-0-1-3-33.
  2. Kablov E.N. Materialy i khimicheskie tekhnologii dlya aviatsionnoy tekhniki [Materials and chemical technologies for aviation engineering] // Vestnik Rossiyskoy akademii nauk. 2012. T. 82. №6. S. 520–530.
  3. Kablov E.N. Aviakosmicheskoe materialovedenie [Aerospace materials science] // Vse materialy. Entsiklopedicheskiy spravochnik. 2008. №3. S. 2–14.
  4. Kablov E.N. Tendentsii i orientiry innovatsionnogo razvitiya Rossii [Tendencies and reference points of innovative development of Russia]: sb. nauch.-inform. mater. 3-e izd. M.: VIAM, 2015. 720 s.
  5. Petrova G.N., Rumyanceva T.V., Beyder E.Ya. Vliyanie modificiruyushhih dobavok na pozharobezopasnye svojstva i tehnologichnost polikarbonata [Influence of modifying additives on fireproof properties and technological effectiveness of polycarbonate] // Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2013. №6. St. 06. Available at: http://www.viam-works.ru (accessed: July 25, 2016).
  6. Barbotko S.L. Pozharobezopasnost aviacionnyh materialov [Fire safety of aviation materials] // Aviacionnye materialy i tehnologii. 2012. №S. S. 431–439.
  7. Platonov M.M., Larionov S.A. Issledovanie fazovyh perehodov i struktury polimernyh poroshkovyh kompozicij na osnove polidodekalaktama, poluchennyh metodom kristallizacii iz rastvorov v poljarnyh aprotonnyh rastvoriteljah [Investigation of phase transitions and structure of the polymer powder compositions based on polydodecanolactam obtained by crystallization from solutions in polar aprotic solvents] // Aviacionnye materialy i tehnologii. 2016. №S1 (43). S. 65–73. DOI: 10.18577/2071-9140-2016-0-S1-65-73.
  8. Huang S.H., Liu P., Mokasdar A., Hou L. Additive manufacturing and its societal impact: a literature review // Int. J. Adv. Manuf. Technol. 2013. Vol. 67. P. 1191–1203. DOI: 10.1007/s00170-012-4558-5.
  9. Bikas H., Stavropoulos P., Chryssolouris G. Additive manufacturing methods and modeling approaches: a critical review // Int. J. Adv. Manuf. Technol. 2016. Vol. 83. P. 389–405. DOI: 10.1007/s00170-015-7576-2.
  10. Novakova-Marcincinova L., Kuric I. Basic and Advanced Materials for Fused Deposition Modeling Rapid Prototyping Technology // Manuf. and Ind. Eng. 2012. Vol. 11 (1). P. 24–27.
  11. Hill N., Haghi M. Deposition direction-dependent failure criteria for fused deposition modeling polycarbonate // Rapid Prototyping Journal. 2014. Vol. 20/3. P. 221–227. DOI: 10.1108/RPJ-04-2013-0039.
  12. Goodridge R.D., Tuck C.J., Hague R.J.M. Laser sintering of polyamides and other polymers // Progress in Materials Science. 2012. Vol. 57. P. 229–267. DOI: 10.1016/j.pmatsci.2011.04.001.
  13. Kruth J.-P., Levy G., Klocke F., Childs T.H.C. Consolidation phenomena in laser and powder-bed based layered manufacturing // Annals of the CIRP. 2007. Vol. 56/2. P. 730–759. DOI: 10.1016/j.cirp.2007.10.004
  14. Process for the manufacture of polyamide 12 powder with a high melting point: pat. CA 2498712 C; publ. 15.06.10.
  15. Use of a polyamide 12 for selective laser sintering: pat. EP 0911142 B1; publ. 03.08.05.
  16. Method of selective laser sintering with improved materials: pat. US 7794647 B1; publ. 14.08.06.
  17. Seltzera R., De la Escalerab F.M., Seguradoa J. Effect of water conditioning on the fracture behavior of PA12 composites processed by selective laser sintering // Materials Science and Engineering A. 2011. Vol. 528. P. 6927–6933. DOI: 10.1016/j.msea.2011.05.045.
  18. Schmid M., Amado A., Wegener K. Polymer Powders for Selective Laser Sintering (SLS) // 30th International Conference of the Polymer Processing Society. Cleveland, Ohio, 2014. P. 7–12.
  19. Tager A.A. Fiziko-himija polimerov [Fiziko-himiya polymers]. 4-e izd., pererab. i dop. M.: Nauchnyj mir. 2007. 573 s.
  20. Harakteristiki poroshkovoj kompozicii RA 2200 [Characteristics of powder composition of PA 2200] // e-Manufacturing solutions: katalog materialov kompanii EOS. Available at: http://eos.materialdatacenter.com/eo/ (accessed: July 26, 2017).
  21. Harakteristiki poroshkovoj kompozicii PA-12 AdSint [Characteristics of powder composition of PA-12 AdSint] // Material for additive manufacturing: katalog materialov kompanii ADVANC3D Materials® GmbH. Available at: http://www.advanc3dmaterials.com/assets/presentation-sls.pdf (accessed: July 26, 2017).
  22. Harakteristiki poroshkovoj kompozicii FS3200PA [Characteristics of powder composition of FS3200PA] // Farsoon technologies: katalog materialov kompanii Human Farsoon High-tech Co. Ltd. Available at: http://www.farsoon.us/wp-content/uploads/2015/04/3200PA_Specs.pdf (accessed: July 26, 2017).