The irreversible structural modifications of single crystals fine structure of Ni-based superalloys at enduring operation of turbine blades
The results of researches of single-crystal rotor blades from cast Ni-based superalloy ZhS32-VI in process of long-time life cycle testing of gas turbine engine (high-pressure turbine) are represented for microstructure and substructure. It is shown that precipitation of TCP-phases particles in the alloy during high-temperature testing is accompanied by the decreasing of crystal lattice constant of γ-solid solution. It is verified by data of x-ray diffraction analysis, x-Ray microanalysis and scanning electron microscopy. The point is proposed that decreasing of alloying element content in the γ-solid solution as result of TCP-phases precipitation (rich with the refractory elements) leads to the fall of the high-temperature resistance of the material. Also, a TCP-phases make negative influence on mechanical properties of the alloy due to the local destruction of coherency for interphase boundaries in zone of development of TCP-phases particles.
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