Determination of sulfur and carbon in the powder of nickel alloys

Alekseev A.V., Rastegayeva G.Yu., Pahomkina T.N.
UDC
669.245
DOI
10.18577/2307-6046-2018-0-11-20-27
Article PDF (Russian) (590.67 KB)
How to cite
Alekseev A.V., Rastegayeva G.Yu., Pahomkina T.N. Determination of sulfur and carbon in the powder of nickel alloys // Proceedings of VIAM. 2018. No. 11. DOI: 10.18577/2307-6046-2018-0-11-20-27. URL: https://test.viam.ru/en/journal/2018/11/3
Keywords
powder metallurgy, nickel alloys, sulfur determination, carbon determination, infrared absorption spectroscopy method.
Abstract

The sulfur and carbon content in the powders of nickel alloys EP648, VPr50 and VZH159 was determined by combustion in an induction furnace gas analyzer CS-444 company Leco, followed by detection in the infrared cell of the spectrometer. Various catalysts – tungsten with tin, vanadium oxide, copper chips were used for the complete extraction of the elements to be determined and the most suitable of them was chosen. The correct determination of sulfur and carbon is confirmed by the analysis of a standard sample of the nickel alloy composition.

Reference list
  1. Kablov E.N. Innovacionnye razrabotki FGUP «VIAM» GNC RF po realizacii «Strategicheskih napravlenij razvitiya materialov i tehnologij ih pererabotki na period do 2030 goda» [Innovative developments of FSUE «VIAM» SSC of RF on realization of «Strategic directions of the development of materials and technologies of their processing for the period until 2030»] // Aviacionnye materialy i tehnologii. 2015. №1 (34). S. 3–33. DOI: 10.18577/2071-9140-2015-0-1-3-33.
  2. Kablov E.N., Titov V.I., Gundobin N.V., Karpov Y.A., Karfidova K.E., Kudryavtseva G.S. Rhenium and Ruthenium Determination in Nanostructured High_Temperature Alloys for Aerospace Engineering // Inorganic materials. 2015. Vol. 51. No. 14. P. 1363–1369.
  3. Buyakina A.A., Letnikov M.N., Efimochkin I.Yu. Vlyainiye parametrov mekhanicheskogo legirovaniya na morfologiyu chastits metallokeramicheskoy poroshkovoy kompozitsii VZh175+TiCN [The influence of the mechanical alloying parameters on the particles morphology of the metalceramiс powder composition made from VZh175 alloy with TiCN nanopowder] // Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2017. №9. St. 04. Available at: http://www.viam-works.ru (accessed October 21, 2018). DOI: 10.18557/2307-6046-2017-0-9-4-4.
  4. Evgenov A.G., Shcherbakov S.I., Rogalev A.M. Oprobovaniye poroshkov zharoprochnykh splavov EP718 i EP648 proizvodstva FGUP «VIAM» dlya remonta detaley GTD metodom lazernoy gazoporoshkovoy naplavki [Testing EP718 and EP648 superalloys powders produced by FSUE «VIAM» for repair of gas turbine engine components using laser-powder braze] // Aviacionnyye materialy i tehnologii. 2016. №S1 (43). S. 16–23. DOI: 10.18577/2071-9140-2016-0-S1-16-23.
  5. Shestakova E.A., Shaykhutdinova E.F., Yanbayev R.M. Tekhnologii selektivnogo spekaniya dlya aviastroyeniya [Technologies for selective sintering for aircraft industry] // Polzunovskiy almanakh. 2014. №2. S. 21–24.
  6. Kablov E.N. Materialy i tekhnologii VIAM dlya «Aviadvigatelya» [Materials and technologies of VIAM for Aviadvigatel] // Permskiye aviatsionnyye dvigateli: inform. byul. 2014. №S. S. 43–47.
  7. Volosova M.A., Okunkova A.A. Puti optimizatsii protsessa selektivnogo lazernogo plavleniya pri pomoshchi strategii obrabotki lazernym luchom [Ways to optimize the process of selective laser melting using a laser beam processing strategy] // Izvestiya Samarskogo nauchnogo tsentra Rossiyskoy akademii nauk. 2012. T. 14. №4 (2). S. 587–591.
  8. Mazalov I.S., Evgenov A.G., Prager S.M. Perspektivy primeneniya zharoprochnogo strukturnostabilnogo splava VZh159 dlya additivnogo proizvodstva vysokotemperaturnyh detalej GTD [Perspectives of heat resistant structurally stable alloy VZh159 application for additive production of high-temperature parts of GTE] // Aviacionnye materialy i tehnologii. 2016. №S1. S. 3–7. DOI: 10.18577/2071-9140-2016-0-S1-3-7.
  9. Tsao G., Van I. Nanostruktury i nanomaterialy: sintez, svoystva i primeneniye [Nanostructures and nanomaterials: synthesis, properties and applications]. M.: Nauchnyy mir, 2012. 515 s.
  10. Evgenov A.G., Nerush S.V., Vasilenko S.A. Poluchenie i oprobovanie melkodispersnogo metallicheskogo poroshka vysokohromistogo splava na nikelevoj osnove primenitelno k lazernoj LMD-naplavke [The obtaining and testing of the fine-dispersed metal powder of the high-chromium alloy on nickel-base for laser metal deposition] // Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2014. №5. St. 04. Available at: http://www.viam-works.ru (accessed: July 05, 2018). DOI: 10.18577/2307-6046-2014-0-5-4-4.
  11. Kablov E.N., Chabina E.B., Morozov G.A., Muravskaya N.P. Otsenka sootvetstviya novykh materialov s ispolzovaniyem SO i MI vysokogo urovnya [Conformity assessment of new materials using high-grade CO and MI] // Kompetentnost. 2017. №2. C. 40–46.
  12. GOST 6689.18–92. Nikel, splavy nikelevyye i medno-nikelevyye. Metody opredeleniya sery [State Standard 6689.18–92. Nickel, nickel and copper-nickel alloys. Methods for the determination of sulfur]. M.: Gosstandart, 1992. S. 4.
  13. GOST 6689.10–92. Nikel, splavy nikelevyye i medno-nikelevyye. Metody opredeleniya ugleroda [State Standard 6689.10–92. Nickel, nickel and copper-nickel alloys. Methods for determining carbon]. M.: Gosstandart, 1992. S. 4.
  14. GOST 24018.7–91. Splavy zharoprochnyye na nikelevoy osnove. Metody opredeleniya ugleroda [State Standard 24018.7–91. Alloys heat-resistant on a nickel basis. Methods for determining carbon]. M.: Izd-vo standartov, 1991. S. 3.
  15. GOST 24018.8–91. Splavy zharoprochnyye na nikelevoy osnove. Metody opredeleniya sery [State Standard 24018.8–91. Alloys heat-resistant on a nickel basis. Methods for the determination of sulfur]. M.: Izd-vo standartov, 1991. S. 3.
  16. ASTME E1019-11. Standard Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel, Iron, Nickel, and Cobalt Alloys by Various Combustion and Fusion Techniques. ASTM International, 2011. P. 24.
  17. Alekseev A.V., Rastegaeva G.Yu., Pakhomkina T.N. Opyt opredeleniya ugleroda, sery, kisloroda i azota v splavakh na osnove niobiya na gazoanalizatorakh firmy Leco [Experience of the determination of carbon, sulfur, oxygen and nitrogen in alloys based on niobium on the gas-analyzers of the Leco firm] // Trudy VIAM: elektron. nauch.-tehnich. zhurn. 2018. №1. St. 03. URL: http://www.viam-works.ru (accessed: July 05, 2018). DOI: 10.18557/2307-6046-2018-0-1-3-3.