Heat treatment and its influence on the structure and performance characteristics of high strength high-nitrogen martensitic structural steel

Dulnev K.V., Sevalnev G.S., Ulyanov E.I., Oblivantsev K.D.
Dulnev K.V., Sevalnev G.S., Ulyanov E.I., Oblivantsev K.D. Heat treatment and its influence on the structure and performance characteristics of high strength high-nitrogen martensitic structural steel // Proceedings of VIAM. 2026. No. 3. DOI: 10.18577/2307-6046-2026-0-3-23-32. URL: https://test.viam.ru/en/journal/2026/3/2
Keywords
high nitrogen steels, super-equilibrium nitrogen content, heat treatment, microstructure, hardness, construction steel
Abstract

The work studies the microstructure, hardness, and tribological properties of a high-strength, high-nitrogen, martensitic-class structural steel. It has been found that the steel's structure consists of martensite, residual austenite, and excess nitride phases. The steel's hardness on the Rockwell scale ranges from 48,5 to 52,5 HRC, and on the Vickers scale it ranges from 580 to 640 HV5. Tribological tests were conducted, resulting in a minimum average coefficient of friction of 0,45 and a minimum wear rate of 0,7∙10-4 mm3/(N∙m).

Reference list
  1. Kablov E.N. What to Make the Future of? New-Generation Materials, Technologies for Their Creation and Processing ‒ the Basis of Innovations. Krylya Rodiny, 2016, no. 5, pp. 8–18.
  2. Kablov E.N. New-Generation Materials ‒ the Basis of Innovations, Technological Leadership, and National Security of Russia. Intellekt i tekhnologii, 2016, no. 2 (14), pp. 16–21.
  3. Kablov E.N. New-Generation Materials and Digital Technologies for Their Processing. Vestnik Rossiyskoy akademii nauk, 2020, vol. 90, no. 4, pp. 331–334.
  4. Kablov E.N., Bakradze M.M., Gromov V.I., Voznesenskaya N.M., Yakusheva N.A. New high strength structural and corrosion-resistant steels for aerospace equipment developed by FSUE «VIAM» (review). Aviacionnye materialy i tehnologii, 2020, no. 1 (58), pp. 3–11. DOI: 10.18577/2071-9140-2020-0-1-3-11.
  5. Terent’ev V.F., Prosvirnin D.V., Seval’neva T.G. et. al. Structural state and mechanical behavior of Fe–Cr–Ni maraging steels. Russian metallurgy (Metally), 2020, vol. 2020, is. 4, pp. 426–433.
  6. Goncharevskaya D.A. Chemical-thermal treatment of steels with super-equilibrium nitrogen concentration. Politekhnicheskiy molodezhnyy zhurnal, 2020, no. 8 (49). DOI: 10.18698/2541-8009-2020-08-636.
  7. Blinov V.M., Lukin E.I., Blinov E.V. et al. Tensile Fracture of Austenitic Corrosion-Resistant Steels with an Overequilibrium Nitrogen Content and Various Vanadium Contents. Russian Metallurgy (Metally), 2021, vol. 2021, is. 10, pp. 1265–1269. DOI: 10.1134/S0036029521100062.
  8. Rashev Ts.V. High-nitrogen steels. Pressure metallurgy. Sofia: Prof. Marin Drinov, 1995, 272 p.
  9. Gromov V.I., Yakusheva N.A., Vostrikov A.V., Cherkashneva N.N. High strength structural steels for gas-turbine engine shafts (review). Aviation materials and technology, 2021, no. 1 (62), pp. 3‒12. Available at: http://www.journal.viam.ru (accessed: June 25, 2025). DOI: 10.18577/2713-0193-2021-0-1-3-12.
  10. Kablov E.N. Innovative developments of FSUE «VIAM» SSC of RF on realization of «Strategic directions of the development of materials and technologies of their processing for the period until 2030». Aviacionnye materialy i tehnologii, 2015, no. 1 (34), pp. 3–33. DOI: 10.18577/2071-9140-2015-0-1-3-33.
  11. Gudremon E. Special steels. Second ed. Trans. from Germ. Moscow: Metallurgiya, 1966, 1274 p.
  12. Bakradze M.M., Voznesenskaya N.M., Leonov A.V., Krylov S.A., Tonysheva O.A. Development and research of high-strength corrosion-resistant steel for bearing parts. Metallurg, 2019, no. 11, pp. 39–44.
  13. Trojahn W., Streit E., Chin H., Ehlert D. Progress in bearing performance of advanced nitrogen alloys stainless steel, Cronidur 30. Bearing steels: into the 21-st century: ASTM STP 1327 / eds. J.J.C. Hoo, W.B. Green. American Society for Testing Material, 1998, 440 р.
  14. Vostrikov A.V., Sevalnev G.S., Bannykh I.O., Vlasov I.I., Romanenko D.N., Dulnev K.V. Microstructure, hardness and tribotechnical properties evolution of economically alloyed high nitrogen martensitic steel. Trudy VIAM, 2022, no. 9 (115), pp. 3‒14. Available at: http://www.viam-works.ru (accessed: July 01, 2025). DOI: 10.18577/2307-6046-2022-0-9-3-14.
  15. Sevalnev G.S., Gromov V.I., Dulnev K.V., Sevalneva T.G. Contact endurance of nitrogenous austenitic-martensitic steels with different hardening mechanism. Aviation materials and technologies, 2024, no. 2 (75), pp. 3‒14. Available at: http://www.journal.viam.ru (accessed: June 25, 2025). DOI: 10.18577/2713-0193-2024-0-2-3-14.
  16. Krylov S.A., Makarov A.A., Druzhnov M.A. Study of high-strength low-alloy steel with super-equilibrium nitrogen content. Trudy VIAM, 2020, no. 12 (94), pp. 3‒13. Available at: http://www.viam-works.ru (accessed: July 01, 2025). DOI: 10.18577/2307-6046-2020-0-12-3-13.